Parr-instrument Series 4560 Manual de usuario

396M4560Mini Bench Top ReactorsOperating Instruction Manual

Mini Bench Top ReactorsParr Instrument Company10Other Vessel Head Fittings Safety Rupture DiscThere is a safety rupture disc attached to the head whic

Mini Bench Top Reactorswww.parrinst.com11How to Use the VesselRemovable Vessels Always remove removable vessels from the support stand before attempti

Mini Bench Top ReactorsParr Instrument Company12Pressurizing the Vessel Check all valves carefully before admitting gas into the system. The liquid s

Mini Bench Top Reactorswww.parrinst.com13Air MotorVariable speeds from 100 to 2000 rpm with no spark hazard can be obtained by replacing the standard

Mini Bench Top ReactorsParr Instrument Company141. The MotorThe standard variable speed motor is not explo-sion proof, yet these motors are not undul

Mini Bench Top Reactorswww.parrinst.com15Periodic Pressure TestsEach cylinder used in a Parr stirred reactor is tested under hydrostatic pressure to

Mini Bench Top ReactorsParr Instrument Company16General Maintenance Notes1. Periodically inspect all electrical wiring and pres-sure connections for

Mini Bench Top Reactorswww.parrinst.com174560 Series Reaction Vessel Parts ListStandard Vessel Fittings(3000 psig/ 350°C)Consult the itemized list for

Mini Bench Top ReactorsParr Instrument Company18Split Rings and AccessoriesPart No. Description CodeA455HC Split Ring Assembly w/ bolts RV FG454HC Com

Mini Bench Top Reactorswww.parrinst.com19Stirrer Support BracketPart No. Description CodeA1260HC Stirrer Bracket w/ bushing SSA1260HC2* Stirrer Bracke

Mini Bench Top ReactorsParr Instrument Company2Table of ContentsPrefaceScope — 3Related Instructions — 3Safety Information — 3General Specifi cations —

Mini Bench Top ReactorsParr Instrument Company20External FittingsPart No. DescriptionA888HC2 Rupture disc assembly49HC2 Orifice cone527HC Orifice ring

Mini Bench Top Reactorswww.parrinst.com21Digitally signed by Vern Moon4563 Gas Entrainment Assembly600mL Removable VesselNOTE:TEMP DIP TUBES USE A187

Mini Bench Top ReactorsParr Instrument Company22Vessel Closure and Standard Internal Parts*Special Materials4560 Series Reaction Vessel Parts ListHigh

Mini Bench Top Reactorswww.parrinst.com23* For Special FittingsGaskets*Part No. Description Code457HC3KL Head Gasket, Flexible Graphite RV FG48HC Gask

Mini Bench Top ReactorsParr Instrument Company24External FittingsPart No. DescriptionA888HC2 Rupture disc assembly49HC2 Orifice cone527HC Orifice ring

Mini Bench Top Reactorswww.parrinst.com25Overarm Parts ListMotorPart No. Description1355EES Motor VS/PM130VDC 1/8 HPA1554EES Motor VS/PM 130VDC 1/8 HP

Mini Bench Top ReactorsParr Instrument Company26Bomb Support Stand with Fixed Head and 1/8 hp Stirrer Drive MotorA2262EA2179HC PULLEY ASS’Y:

Mini Bench Top Reactorswww.parrinst.com27Bomb Support Stand with Moveable Vessel and 1/4 hp Stirrer Drive Motor

Revision 05/29/13

Mini Bench Top Reactorswww.parrinst.com3PrefaceScopeThese instructions describe the installation, op-eration and maintenance of Parr Series 4560 Mini

Mini Bench Top ReactorsParr Instrument Company4Explanation of SymbolsII On position, full power heater switchI On position, half power heater switchO

Mini Bench Top Reactorswww.parrinst.com5User’s ResponsibilityAll Parr reactors and pressure vessels are designed and manufactured with great care to a

Mini Bench Top ReactorsParr Instrument Company6Parr Series 4560 Mini Reactors are furnished with two structural options in addition to the size, press

Mini Bench Top Reactorswww.parrinst.com7InstallationPressure and Temperature LimitsThe working pressure and temperature at which any reactor or pressu

Mini Bench Top ReactorsParr Instrument Company8Assemble the ReactorThese reactors require at least 10 sq. ft. of work-space in a well-ventilated area

Mini Bench Top Reactorswww.parrinst.com910. Note the voltage and amperage requirement stamped on the controller data plate, and then plug the power co